1H-X Correlation

From $375.00*

Pines Magnetic Resonance Center (PMRC) - Core NMR Facility

5 days

2D 1H-X correlation spectroscopy for various nuclei other than 13C (e.g. 31P, 29Si, 15N, etc.) at 500 MHz or higher and T=298 K. Please consult with NMR staff about project details.

The facility can provide the following services: sample preparation (i.e. dissolution, packing rotors); routine data collection, processing and analysis. If requested, an NMR Report will be generated which will contain a brief experimental statement, and the spectrum or spectra consistent with the complexity of the experiment requested. All data will be stored on secure servers, unless otherwise requested, and all data will be accessible online by the customer via email or secure file transfer protocols of their choice.

The NMR staff will endeavor to complete any and all services requested and accepted within 5 days of receipt of the sample from the customer; however, due to the inherent variability of the schedule involved in the operation of an open access core facility, this time frame cannot be guaranteed. Sample status will be communicated to the customer user as updates are available. Final data will be transmitted to customer as soon as it is available.

Pricing is dependent on the sample concentration and additional handling instructions as needed. Please request a quote for an accurate cost estimate. Instrument hourly rate: $90, Staff hourly rate: $285.

Submission Guideline

NOTE: Access to UC Berkeley facilities and services requires university approval which takes as little as fast as 24 hours. First time customers on Second Lab will be prompted to complete approval requirements during checkout. We encourage you to book your 15 minute onboarding with the Second Lab team through the following link: Click here to schedule your onboarding (15 mins)!

During checkout, you will be presented with a form for the respective service you're requesting. Additional requirements may be applicable if your service requires physical access to University of California facilities.

FAQs

1) Turnaround time? We run the samples ideally within 24 hours on week days after they arrive, but will send an updated timeline to the customer if more time is necessary. If additional sample preparation work is we will also inform the customer.

2) Expedited services available? Yes, depends on sample and project. Send us a message with your particular requirements.

3) How will results be formatted? The customer will receive raw Bruker data. The FID can be processed using Bruker's Topspin or any other commercially available software package, e.g. Mnova, ACD Labs, etc. Send us a message if additional processing assistance is needed.

4) Can I request any unprocessed samples be returned to me? Yes, we just need you to provide shipping labels or pick up in person. Send us a message to arrange returns.

Lab Information

Pines Magnetic Resonance Center (PMRC) - Core NMR Facility

College of Chemistry, University of California, Berkeley, Gilman Hall, California

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